Nanoindenter Hystron TI 950 TriboIndenter
Transducer Calibration
Sets the force constant of the load and displacement transducers.
- Calibration tab → System Calibrations (standard)
- Ensure calibration constants for indentation axis match the numbers on the wall.
- Once set, press "calibrate" and select "do cal air indent"
Workspace / Sample Definition
Sets boundary of the sample so you can navigate easily.
- Calibration tab → Stage Calibration (or sample navigation tab)
- Create a new sample (can't overlap an old sample)
- Move the crosshairs over the corners of the sample and select "Pos. Add" for all 4 corners
Tip to optic calibration
To set the z offset between the sample and objective.
- Calibration tab → Stage Calibration → "Slot 1 Tip to Optic Calibration"
- Select "H-pattern" button
- Focus on location you'd like to place the H pattern.
- Next, it will ask to do a manual approach and bring the tip down to ~1mm above the sample
- Risk of Crashing if you don't pay attention here
- leaving it too high will only increase time required to approach sample. Play it safe.
- Z height for tip to optic calibration of a typical silicon wafer on steel puck = ~49.7 mm
- When about ~1mm above sample, check if the indenter tip is above the location you think it should be
- if it is not, you may need to redo this tip to optic calibration. Instead of starting with "H" pattern, select the "set x and y axis offset to default" button.
- This is a good starting point in case a previous user messed up the offset.
- if it is not, you may need to redo this tip to optic calibration. Instead of starting with "H" pattern, select the "set x and y axis offset to default" button.
- Once done, center on the H pattern.
Automating Acquisition
Can select locations to test and select a preloaded loading program for each location.
- Don't run a Method chain with the same method back-to-back or else it won't loop through them. It will stop after the first iteration. Need to have the cycle repeat.
- i.e. 123451234512345 instead of 111222333444555
Creating Method
Setting Indentation Locations
Setting Load Function
Manual:
, multiple selections available,