Nanoindenter Hystron TI 950 TriboIndenter
Transducer Calibration
Sets the force constant of the load and displacement transducers.
Calibration tab → System Calibrations (standard)
Ensure calibration constants for indentation axis match the numbers on the wall.
Once set, press "calibrate" and select "do cal air indent"
Workspace / Sample Definition
Sets boundary of the sample so you can navigate easily.
Calibration tab → Stage Calibration (or sample navigation tab)
Create a new sample (can't overlap an old sample)
Move the crosshairs over the corners of the sample and select "Pos. Add" for all 4 corners
Tip to optic calibration
To set the z offset between the sample and objective.
Calibration tab → Stage Calibration → "Slot 1 Tip to Optic Calibration"
Select "H-pattern" button
Focus on location you'd like to place the H pattern.
Next, it will ask to do a manual approach and bring the tip down to ~1mm above the sample
Risk of Crashing if you don't pay attention here
leaving it too high will only increase time required to approach sample. Play it safe.
Z height for tip to optic calibration of a typical silicon wafer on steel puck = ~49.7 mm
When about ~1mm above sample, check if the indenter tip is above the location you think it should be
if it is not, you may need to redo this tip to optic calibration. Instead of starting with "H" pattern, select the "set x and y axis offset to default" button.
This is a good starting point in case a previous user messed up the offset.
Once done, center on the H pattern.
Automating Acquisition
Can select locations to test and select a preloaded loading program for each location.
Don't run a Method chain with the same method back-to-back or else it won't loop through them. It will stop after the first iteration. Need to have the cycle repeat.
i.e. 123451234512345 instead of 111222333444555
Creating Method
Setting Indentation Locations
Setting Load Function