Photoluminescence
Safety
Always wear laser safety goggles when using the laser, make sure that you have the correct goggles for the wavelength range of the laser
Turn on the laser warning light indicator
In any setup make sure that the beam path is terminated at the beam dump and also make sure there are not stray reflections
Always place the beam block in front of the laser before making any changes to the optical beam path, this includes changing samples
Components
532nm DPSS pump laser
Since this laser does not have a built in power meter check the laser output power using the bolometer. While measuring power do not chop the beam.
532nm narrow bandpass filter to eliminate other wavelengths coming from the laser.
optical chopper: improves signal to noise ratio (SNR).
Detectors
Germanium detector, LN2 cooled to 77K, 500nm to 1500nm, set chopper to 100Hz
InGaAs detector, TE cooled upto -20C, 500nm to 1650nm, set chopper to 350Hz
InSb detector, LN2 cooled to 77K, 1500nm to 8000nm, set chopper to 350Hz
SR830 Lock-in amplifier
Acton SpectraPro 2500i spectrometer (0.5m optical path)
Sample holder
The sample holder is connected to house vacuum. A toggle valve located above the PL setup turns on/off vacuum. Place the sample on the sample holder and turn-on vacuum to hold the sample firmly in place.
It also has precision micrometer to move the sample forwards and backwards for precision alignment.
Software
The most recent software (as of July 2015) is a python GUI application called SimplePL, written by Scott Maddox. It is available on Github.
Setting up a scan
Turn on the laser.
Slowly ramp it up to the desired operating current, wait for the laser output power to stabilize.
Measure the incident power by removing the sample holder and letting the pump beam fall on the bolometer.
Repeat the same, but this time place the sample on the sample holder and the bolometer in the place of the beam dump to measure reflected power.
The difference of the above two powers will give the effective pumping power.
Detector
Attach the appropriate detector at the exit slit of the spectrometer